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Beilstein J. Org. Chem. 2019, 15, 44–51, doi:10.3762/bjoc.15.4
Graphical Abstract
Scheme 1: Strategy for sequential ROMP of 1 to yield 3.
Scheme 2: ROMP of 4 and 5 in THF at 0 °C in the presence of 10 mol % of 6.
Scheme 3: Retrosynthesis of 8 from 9.
Scheme 4: Synthesis of monomer 9.
Scheme 5: Synthesis of 14 and 8 by selective olefin metathesis.
Scheme 6: Cyclopolymerization of 15 with a flexible linker.
Scheme 7: Methanolysis of unsymmetrical ladderphane 8.
Beilstein J. Org. Chem. 2015, 11, 2343–2349, doi:10.3762/bjoc.11.255
Figure 1: Molecular structure of TTF derivatives T1 and T2.
Scheme 1: The synthetic routes of compounds T1 and T2.
Figure 2: SEM images of T1 (a) and T2 (b) films on glass substrates (drop-coated from diluted T1 or T2 soluti...
Figure 3: The UV–vis spectra of T1 (a) and T2 (b) at different concentrations in ethyl acetate.
Figure 4: IR spectra of (a) T1, (b) T2, (c) TCNQ, (d) T2/TCNQ, and (e) T1/TCNQ.
Figure 5: (a) UV–vis spectra of T1 solutions TCNQ and T1/TCNQ in ethyl acetate (1 × 10−3 M). (b) UV–vis spect...
Figure 6: Cyclic voltammograms of T1 and T2 in DCM. Conditions: 0.1 M tetrabutylammonium hexafluorophosphate,...
Figure 7: Cyclic voltammograms of T1 and TCNQ in DCM. Conditions: 0.1 M tetrabutylammonium hexafluorophosphat...